李贺 19112211实验：连续均相反应器停留时间分布的测定实验装置及流程：实验数据记录流量：20L/H 示踪剂注入量：3ml釜ABC单釜平均t/s100.81182.9293.68139.4方差0.760.310.010.6釜数1.313.2678.281.66流量：20L/H 示踪剂注入量：4ml釜ABC单釜平均t/s113.96190.5322.44149.18方差0.720.28-0.050.52釜数1.393.52-21.61.91流量：15L/H 示踪剂注入量：4ml流量：15L/H 示踪剂注入量：3ml实验：液固催化反应动力学测定温度/初始PH初始碱浓度/(mol/L)NaOH流量/(m3/h)酯流量/(m3/h)最终PH最终碱浓度/(mol/L)27.411.850.0070794584.28.8210.440.00027542311.850.0070794585.2511.1310.690.00048977911.850.0070794586.5113.8610.850.00070794637.511.850.0070794584.28.8210.260.0001819711.850.0070794585.2511.1310.420.00026302711.850.0070794586.5113.8610.540.00034673735.012.10.0125892545.2511.1310.420.00026302712.10.0125892546.5113.8610.540.00034673745.011.80.0063095734.28.829.948.70964E-0511.580.0038018945.2511.539.999.77237E-0511.580.0038018946.5113.869.989.54993E-0555.010.90.0007943284.28.827.442.75423E-0710.880.0007585785.2511.537.11.25893E-0710.840.0006918316.5113.866.918.12831E-08温度/CA0/CAtk27.425.703957837.33333E-0561000014.454397715.86667E-05104.73118E-0535.047.863009235.86667E-05100000036.307805484.73118E-0537.538.90451457.33333E-0572000026.915348045.86667E-0520.417379454.73118E-0545.072.443596017.33333E-05130000038.90451455.86667E-0539.810717064.73118E-0555.02884.0315037.33333E-05-2200000006025.5958615.86667E-058511.3803824.73118E-05温度T/K温度倒数1/T(K-1)klnk300.550.00332723361000013.32121424308.150.003245173100000013.81551056310.650.00321905772000013.48700649318.150.003143171130000014.07787482328.150.003047387-220000000无解实验：气升式环流反应器流体力学及传质性能的测定H0=942mmH=948mm时间t/s流量L/(kg/h)导电率时间t/s流量L/(kg/h)导电率020000.1291420000.1540.520000.12914.520000.156120000.1041520000.1561.520000.10415.520000.156220000.1041620000.1632.520000.08616.520000.163320000.0861720000.1693.520000.13517.520000.169420000.1351820000.1684.520000.21318.520000.168520000.2131920000.1665.520000.20419.520000.166620000.2042020000.1616.520000.18220.520000.161720000.1822120000.1627.520000.13721.520000.162820000.1372220000.1648.520000.14422.520000.164920000.1442320000.1669.520000.16123.520000.1661020000.1612420000.16610.520000.18124.520000.1661120000.1812520000.16411.520000.17725.520000.1641220000.1772620000.16312.520000.16426.520000.1631320000.1642720000.16313.520000.154时间t/s电压U/VUmax-U*ln(Umax-U*)/(Umax-U)时间t/s电压U/VUmax-U*ln(Umax-U*)/(Umax-U)83.411.9012310.84.50.9724610038.53.411.90123.510.84.50.97246100393.511.80.00843886912410.84.50.9724610039.53.511.80.008438869124.510.74.60.950482097103.611.70.01694955812510.74.60.95048209710.53.611.70.016949558125.510.74.60.950482097113.611.70.01694955812610.74.60.95048209711.53.611.70.016949558126.510.64.70.928975891123.611.70.01694955812710.64.70.92897589112.53.411.90127.510.74.60.950482097133.411.9012810.74.60.95048209713.53.611.70.016949558128.510.94.40.994933859143.611.70.01694955812910.94.40.99493385914.53.611.70.016949558129.510.94.40.994933859153.611.70.01694955813010.84.50.97246100315.53.711.60.025533302130.510.84.50.972461003163.711.60.02553330213110.94.40.99493385916.53.611.70.016949558131.510.94.40.994933859173.611.70.016949558132114.31.01792337717.53.611.70.016949558132.5114.31.017923377183.611.70.01694955813311.14.21.04145387518.53.611.70.016949558133.511.14.21.041453875193.611.70.01694955813411.24.11.06555142619.53.811.50.034191365134.511.24.11.065551426203.811.50.03419136513511.24.11.06555142620.53.711.60.025533302135.511.24.11.065551426213.711.60.02553330213611.24.11.06555142621.53.711.60.025533302136.511.24.11.065551426223.711.60.02553330213711.24.11.06555142622.53.711.60.025533302137.511.24.11.065551426233.611.70.01694955813811.24.11.06555142623.53.611.70.016949558138.511.24.11.065551426243.711.60.025533302